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publicationDate 2008-09-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber EC-SP088679-A
titleOfInvention PROCESS FOR THE PREPARATION OF DIBENZOTIAZEPINE COMPOUNDS
abstract A di-benzothiazepine compound is appropriately prepared by subjecting a 2-amino-2'-carboxy-diphenylsulfuroid compound to dehydration-condensation reaction in the presence of an acid catalyst; the 2-amino-2'-carboxy-diphenylsulfide compound is appropriately prepared by reducing the 2-nitro-2'-carboxy-diphenylsulfide compound in a lower aliphatic ester solvent; and the 2-nitro-2'-carboxy-diphenylsulfide compound is appropriately prepared by reacting a nitrobenzene compound with a thiosalicylic acid compound in a mixture of a lower aliphatic alcohol and water.
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Total number of triples: 28.