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publicationDate 1992-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DE-4202262-A1
titleOfInvention METHOD FOR PRODUCING 2-NITRO-5-PHENYLTHIOANILINE
abstract Prepn. of 2-nitro-5-phenylthioaniline (I) comprising reaction of 5-chloro-2-nitroaniline (II) with thiophenol in the presence of an alkaline alkali metal cpd. pref. hydroxide, pref. in aq. soln. in the presence of organic solvent at room temp. or higher; sepg. the inorganic cpd.; and removing the organic solvent and purifying by crystallisation is characterised in that: the reaction is in the presence of halide and linear or cyclic polyether oxypolyether contg. 6-25 ether gps. in an amt. of 2-15 wt.% based on (II). USE - (I) is an intermediate for phenylguanidine or benzimidazol derivs. useful for treating worm infestations in animals including humans
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