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filingDate 1973-09-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_af23086e4d8cf825745e48b3008d712d
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publicationDate 1974-09-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DE-2345199-A1
titleOfInvention PROCESS FOR THE PREPARATION OF AETHAN1-HYDROXY-1,1-DIPHOSPHONIC ACID
abstract Title cpd is made from phosphorous (III) oxide, phosphoric acid and an acetylating agent, consisting of acetic acid and/or acetic anhydride, and characterized by the phosphorus (III) oxide and phosphoric acid, in molar ratios of 10:1 to 1:10 esp. 2:1 to 1:4, are mixed with acetic acid and acetic anhydride and reacted at a temp. 80-120 degrees C esp. 115 degrees C for 5 min. to 4 hrs. esp. 60 mins, to form partially condensed, partially acetylated ethane hydroxy phosphoric acid, the excess acetylating agent decomposed in a known manner, and by deacetylating at a pressure of 1-250 torr, esp. 10-80 torr, and temp. of 80-200 degrees C, esp. 160-180 degrees C the condensed AEHDP- acids, the acetylating agent was recovered and the condensed acid converted to the monomeric acid in a known manner.
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priorityDate 1973-03-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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