Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5c24684033fba97d1ad845ce453a57e3 |
classificationCPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C45-85 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C43-30 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09B41-00 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09B41-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C47-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-30 |
filingDate |
1971-08-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b705d47a665b3c49f78661087be9b3f7 |
publicationDate |
1973-02-15-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
DE-2139211-A1 |
titleOfInvention |
PROCESS FOR THE ISOLATION OF TRIFLUOROACETALDEHYDE FROM FLUORINATION PRODUCTS OF CHLORAL IN THE FORM OF SEMI-ACETALS |
abstract |
The mixts., obtd. by chloral fluorination, and contg. CF3CHO.HF and HCl are reacted with Si(OR)4 or ROH and SiCl4 to form the hemiacetal of formula:- CF3CH(OH)OR (where R is 1-5C alkyl). The HCl and SiF4 formed are driven off by heating or inert gas and the hermiacetal recovered by fractional distillation. It is a convenient storage stable and transportable form of the aldehyde which is converted to the free aldehyde by reaction with H2SO4 or polyphosphoric acid. |
isCitedBy |
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4480139-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-2007119351-A http://rdf.ncbi.nlm.nih.gov/pubchem/patent/EP-0044650-A1 http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-4523038-A |
priorityDate |
1971-08-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |