http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DE-19636191-B4

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filingDate 1996-09-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2008-04-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_df1dc58f1de34786ed91d2bac014e0e0
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publicationDate 2008-04-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DE-19636191-B4
titleOfInvention Process for the purification and concentration of used sulfuric acids
abstract A process for purifying and concentrating contaminated sulfuric acids resulting from the nitration of aromatic hydrocarbons in the presence of sulfuric acids, wherein the steam-volatile impurities are completely removed from the sulfuric acid in a purification step and the thus purified sulfuric acid is concentrated a) the sulfuric acid at a temperature of 50 to 180 ° C in countercurrent with water vapor and with vapors from the first concentration stage of steam-volatile impurities at pressures between 200 and 1000 mbar is released, the water vapor in an amount of 10 to 30 wt .-% is added based on the amount of sulfuric acid, b) the sulfuric acid from a) is passed into a first Aufkonzentrierstufe in which it is concentrated under indirect heat at the same pressure as under a) by up to 5 wt .-% and then c) the sulfuric acid from b) is fed to a single or multi-stage vacuum concentration in which the pressure is lower than in b) and the ...
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priorityDate 1996-08-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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