http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DE-1813646-A1

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ef819c886fac1a8b82ad8cd254f58a7a
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C309-00
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C309-29
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C309-28
filingDate 1968-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f7a6f0f344786331d80334403c4684a8
publicationDate 1970-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DE-1813646-A1
titleOfInvention Process for the production of arylsulfonic acids
abstract Aryl sulphonic acids are predp. by introducing in each consecutive step, hydrocarbon, pref. benzene, into a mixture of aryl sulphonic acid and conc. H2SO4 from a previous step. Sulphonation temp. is 100-120 degrees C. in the first step, increasing to 180 degrees C. in the last step. Water formed is removed by azeotropic distillation and H2SO4 concentration is adjusted to ensure 50% conversion (calC. on H2SO4 present). Reaction is continued with re-use of hydrocarbon, after water separation, until over 90% yield arylsulponic acid is obtained.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DE-2353918-A1
priorityDate 1968-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 27.