http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DE-10253094-A1

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publicationDate 2004-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DE-10253094-A1
titleOfInvention Process for the purification of caprolactam
abstract Process for the purification of crude caprolactam obtained by 1) a mixture (I) containing 6-aminocapronitrile and water to a mixture (II) containing caprolactam, ammonia, water, high boilers and low boilers, reacted in the presence of a catalyst, then 2) ammonia removed from mixture (II) to obtain a mixture (III) containing caprolactam, water, high boilers and low boilers, then 3) completely or partially removed from mixture (III) water to give a crude caprolactam (IV) containing caprolactam, high boilers and low boilers, characterized in that one a) the crude caprolactam and an inorganic acid which has a boiling point above the boiling point of caprolactam under the distillation conditions according to the following steps b) to h) are fed to a first distillation device K1, b) the crude caprolactam and the inorganic acid are distilled in the first distillation device K1, a first partial stream in the bottom area and a second partial stream in the top area being removed from the distillation device K1, c) feeding the second partial stream from step b) to a second distillation device K2, d) the second partial stream from step b) is distilled in the second distillation device K2, a first partial stream in the bottom area and a second partial stream in the top area being taken from the distillation device K2, e) the first partial stream from step d) a ...
priorityDate 2002-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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