http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DD-234676-A1
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ad4b55ad0c2b10522c4359cbbdb8971d |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D221-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D487-08 |
filingDate | 1985-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a62b4877d9a1cb6c1bc1505ddbd2ebde http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b9fcae17f4c68a34556b52bb5a2e18f |
publicationDate | 1986-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | DD-234676-A1 |
titleOfInvention | PROCESS FOR PREPARING 2-ACYL-3-TRICHLOROMETHYL-2-AZANORBORN-5-ENENE |
abstract | The invention relates to a process for the preparation of 2-acyl-3-trichloromethyl-2-azanorborn-5-enes 1, wherein the azomethines 3 are not isolated, but are reacted immediately after formation with 4. This eliminates a complex step associated with yield losses. By addition of traces of hydroquinone to the reaction mixture as a stabilizer as well as by anaerobic procedure, side reactions of the azomethines 3 are minimized by radical processes, thereby increasing the yield. The addition of 0.1 mol% of freshly sublimed aluminum chloride with respect to 2 leads to a further increase in yield. The azanorbornene derivatives 1 are of interest as crop protection and pest control agents or as starting materials for their synthesis. In addition, these derivatives are starting materials for pharmacologically interesting compounds. |
priorityDate | 1985-02-18-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 46.