http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DD-150900-A1

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_22c8b5a03c2a4dc1ef0dd92110a8ec6d
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_6f918f3b9776987c4d43a13cd69b7e2c
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F9-202
filingDate 1980-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1352a80eae765ee2af2fcc0203529a34
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d8438e56e639ccba74d8413394aa781b
publicationDate 1981-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DD-150900-A1
titleOfInvention PROCESS FOR THE PREPARATION OF THIOPHOSPHORIC ACID-O, O-DIALKYLESTER
abstract The invention relates to a one-pot reaction for the preparation of Thiophosphorigsaeure-O, O-dialkyl esters of elemental phosphorus. The aim of the invention is to produce thiophosphoric acid O, O-dialkyl esters in high yields and in tolerable reaction times. According to the invention, elemental white phosphorus is reacted with tetrachloromethane, alcohols, sodium alcoholates and subsequently with hydrogen sulphide in the presence of weak bases as catalysts at temperatures of 0 to 60 ° C. in a solvent or solvent mixture. Thiophosphoric acid O, O-dialkyl esters serve as intermediates in the preparation of insecticides, acaricides and nematicides.
priorityDate 1980-05-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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