http://rdf.ncbi.nlm.nih.gov/pubchem/patent/DD-142879-A5

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_0e77f06144be4708a6ae75bd9fee56a4
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D277-72
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D277-72
filingDate 1979-04-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_efed47205457e0c7873e84d35ad5c6a3
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b899f75ba24a06d0d74ac74eaab833f
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c4b98db40942cd163595748182d4d55c
publicationDate 1980-07-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber DD-142879-A5
titleOfInvention PROCESS FOR THE PREPARATION OF 2-MERCAPTOBENZTHIAZOLE
abstract These compounds are valuable vulcanization accelerators. The aim is to provide a simple and economical process that gives good yields without catalysts at relatively low pressures in shorter reaction times. According to the invention, nitrobenzene or nitrosobenzene, hydrogen sulfide and carbon disulfide are optionally reacted together under pressure, the nitrobenzene / nitrosobenzene / hydrogen sulfide molar ratio being 1: 3 to 1: 6 and 1: 1.5, respectively to 1: 4, the nitrobenzene / nitrosobenzene / carbon disulfide molar ratio 1: 1 to. 1: 3 and the final temperature in the reaction is at least 200 to 300 0C. The reaction is first carried out at temperatures of 150 to 170 0C and then from 200 to 250 0C. The reaction is carried out in particular under the egg-pressure of the reactants. At the final temperature, the reaction pressure is 15 to 65 bar.
priorityDate 1978-04-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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