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filingDate 1990-08-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7f6b152c109e1a6c48a94ab7e3f0f0c3
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publicationDate 1993-06-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CZ-277935-B6
titleOfInvention Method of separating and employing residues from waste water formed during the synthesis of 5-amino-4-chloro-2-phenyl-3(2h)-pyridazinone
abstract A process for the separation and reutilisation of residual substances from the waste water of the synthesis of 5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone I <IMAGE> prepared from 4,5-dichloro-2-phenyl-3(2H)-pyridazinone II <IMAGE> and ammonia, characterised in that the residues of the product I dissolved in the waste water together with the by-products a) 4-amino-5-chloro-2-phenyl-3(2H)-pyridazinone Ia <IMAGE> and b) 4-chloro-5-hydroxy-2-phenyl-3(2H)-pyridazinone Ib <IMAGE> are precipitated and isolated by acidifying the waste water and the mixture thus obtained is converted into 4,5-dichloro-2-phenyl-3(2H)-pyridazinone II using a chlorinating agent.
priorityDate 1989-08-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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