http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CZ-2011152-A3

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d8faf71a78bf0e9b2d4b7357812d84ee
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C381-00
filingDate 2011-03-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4cdb0f50f8a159e6108616e4c7a16803
publicationDate 2011-11-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CZ-2011152-A3
titleOfInvention Process for preparing substituted nitrophenylsulfurpentafluoride
abstract The process for preparing substituted nitrophenylsulfurpentafluoride of formula 2 by substituting a nucleophilic aromatic substitution for hydrogen, wherein the nitrophenylsulfuropentafluoride having a nitro group attached at the meta or para position is reacted in an organic solvent with the compound of formula 3 in the presence of an excess of base and then with an excess of the compound of formula of formula R.sup.3.nXsup.2.n., where R.sup.3.n. is selected from the group consisting of hydrogen, C.sub.1-10.n. alkyl, allyl, or benzyl and X.sup.2. is halogen. The invention includes subsequent chemical modifications of the primary products. This method further comprises reducing the product to aminophenyl sulfurpentafluorides of formula 4 and further converting them with sodium nitrite in the presence of a mineral acid to substituted phenylsulfuropentafluorides of formula 5. Substituents R &lt; 1 &gt;, R &lt; 2 &gt; .3.n., X.sup.1.n. and X.sup.2.n. have the meanings given in the specification.
priorityDate 2011-03-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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