http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CZ-118995-A3

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_acda4db875819409a75c9189cd9127f7
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4ba174d8c5f519b36c907a0f979b7aec
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D295-24
filingDate 1995-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_62a45b195a741bc662eecb6e638b5d4f
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_03c19bf03fb1ec12ca1e2274b3501a4a
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f686990de545c13884eebf734ba0a23e
publicationDate 1996-11-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CZ-118995-A3
titleOfInvention Process for preparing solutions of n-methylmorpholinoxide with a low content of nitrosomorpholine
abstract A method of preparing N-methylmorpholinoxide by oxidising N-methylmorpholine in an aqueous hydrogen peroxide solution at a temperature of 55 to 75 degrees C with a molar ratio of H2O2/amine=0.4 to 0.9, preferably 0.5 to 0.70 possibly in the presence of chelating reagents, possibly in the presence of CO2, with distilling off of unprecipitated N-methylmorpholine under reduced pressure. After adding hydrogen peroxide to the reaction mix and after a decrease in its concentration to 0.05 to 0.15 % of mass, 0.01 to 0.05 % of mass of hydrazine is added, calculated to the reaction mix, and the mixture is kept at reaction temperature for a further half to three hours.
priorityDate 1995-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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