http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CS-215095-B2
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_69c91bbf0395db010b4806f50d808c4e |
classificationIPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K31-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-30 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D213-56 |
filingDate | 1977-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b7503bad7c9de41d2d1f75e3ab25c7c4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_23abeea17488390b2591b34b6dad5ba1 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4b9700327a3adb48a37fbb09f9a220cd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e101f5baa4133229c654e252f063152b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2fe9e928617f4aa6c53839faa732596d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2b406976717e74670c9999cf22827945 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0fc33a0f1559638ec83776e34a430fb1 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f9fa8175a95204b411cd1853e16c1c10 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_74368fa00a25ec5d3b6250caba78ac2e |
publicationDate | 1982-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CS-215095-B2 |
titleOfInvention | Process for preparing 2,6-dihydroxymethylpyridine bis (N-methylcarbamate) |
abstract | The present invention relates to a process for the preparation of 2,6-dihydroxymethylpyridine bis (N-methylcarbamate),nwhich is carried out by allowing it to reactn2,6-dihydroxymethylpyridine hydrochloridenwith tertiary methyl isocyanate, tetrahydrofuran,nacetonitrile or halonhydrocarbon, in the presence of at leastnone equivalent, calculated on the hydrochloride,na tertiary amine, preferably a trialkylaminenor a cyclic tertiary amine,nnitrogen-substituted alkylnwith 1 to 4 carbon atoms, the reaction mixture is stirrednthe crude product is recrystallizednfirst from water, then from the mixturenmethanol or ethanol and water, preparednin a ratio of 1: 1 to 1: 2, this beingnthe mixture is used in four to six timesnamount, calculated on recrystallizednthe product, and the product obtained is dried at room temperaturentemperature of 50 to 100 ° C.n2,6-dihydroxymethylpyridine bis (N-methylcarbamatenis widely used in medicinento treat vascular diseases |
priorityDate | 1976-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 65.