http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-115219541-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N24-087
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C43-13
filingDate 2022-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7c7e57dfc9808e74be79c50c32c15410
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8bff3cdb22a8692e8cee1133015d8df0
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publicationDate 2022-10-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-115219541-A
titleOfInvention A kind of structural analysis method of ethoxylated trimethylolpropane
abstract The present invention provides a method for analyzing the structure of ethoxylated trimethylolpropane, comprising: reacting an ethoxylated trimethylolpropane sample to be analyzed with a derivatization reagent to obtain a derivatized liquid sample; Put the liquid sample into the nuclear magnetic tube, add the deuterated reagent; send the sample dissolved in the deuterated reagent into the nuclear magnetic resonance spectrometer for hydrogen spectrum test, and obtain the hydrogen nuclear magnetic resonance spectrum data; put the obtained sample hydrogen spectrum data After processing and analysis, the baseline was corrected, the peak was determined and the peak was integrated to calculate the molecular weight of the ethoxylated trimethylolpropane and the graft ratio of the terminal hydroxyl group. In the invention, the ethoxylated trimethylolpropane sample is subjected to derivatization pretreatment by acetic anhydride, and combined with the analysis method of hydrogen nuclear magnetic resonance, so as to avoid the terminal hydroxyl group of the ethoxylated trimethylolpropane on the EO chain. Integrated interference from overlapping methyl peaks allows a quick and easy determination of the average molecular weight of ethoxylated trimethylolpropane.
priorityDate 2022-07-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 40.