http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-115057771-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-54
filingDate 2022-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_367f0173e23c3c495467983cb823b693
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f815f591dc7032ebe229abf830d3db79
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publicationDate 2022-09-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-115057771-A
titleOfInvention A kind of method for preparing hexacarboxylic acid ester and novel production process method for preparing adipic acid diester product
abstract A method for preparing hexabasic carboxylic acid ester and a novel production process for preparing adipic acid diester products, the method for preparing hexabasic carboxylic acid ester: A, a hexabasic carboxylic acid composition, an alcohol-containing composition and a catalyst are mixed and added to react The kettle is heated to carry out the reaction; B, add water agent to the reaction solution in step A; C add an alcohol-containing composition to the delighting reaction solution in step B for reaction; and obtain hexavalent carboxylic acid ester through the above steps. The method for preparing an adipic acid diester includes A, mixing an adipic acid composition, an alcohol-containing composition, and an esterification catalyst into a reaction kettle for reaction; B, adding a water-carrying agent to the reaction solution in step A; C dehydrating in step B; Add the alcohol composition to the light reaction solution for reaction; D rectify the reaction solution obtained by the reaction in step C to obtain an adipic acid diester product. The invention provides a method for preparing hexabasic carboxylic acid ester and a method for preparing adipic acid diester with high reaction conversion rate, impurity adipic acid monoester content below 1%, adipic acid diester product yield up to 98% or more, and The reaction conditions are mild and the equipment investment is low.
priorityDate 2022-05-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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