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filingDate 2022-04-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fde313442af8c16f04c91f2007da620e
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publicationDate 2022-08-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114874199-A
titleOfInvention A kind of method for preparing epoxy hesperetin and epoxy bergamot simultaneously
abstract The invention provides a method for simultaneously preparing epoxy hesperidin and epoxy bergamot, comprising: mixing pomelo peel powder with petroleum ether, ultrasonic-assisted extraction, suction filtration, concentration and drying to obtain a crude extract; The crude extract is dissolved in petroleum ether, separated by rapid preparative liquid phase, and purified by semi-preparative liquid chromatography, and the target components are collected according to the spectrum collected by the chromatographic detector to obtain peak 1 and peak 2 of the target components; The target component peaks 1 and 2 were identified by nuclear magnetic resonance and mass spectrometry, and it was determined that the target component peak 1 was epoxy hesperetin, and the target component peak 2 was epoxy bergamot. Thus, high-purity epoxy bergamot and epoxy hesperetin can be rapidly purified and prepared at the same time.
priorityDate 2022-04-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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