abstract |
The invention relates to a method for rapidly synthesizing N-1-naphthylethylenediamine hydrochloride by a microwave-assisted one-pot method. In this method, a self-made atomizer is used to spray the liquid 1-chloronaphthalene onto the solid surface of ethylenediamine hydrochloride to make it fully contact and react under microwave radiation, and this method adopts a one-pot synthesis method, which does not produce intermediate products and has the advantages of The reaction equipment is simple, easy to operate, and has the characteristics of high yield. The whole process does not add any catalyst, and has the advantages of green and pollution-free. |