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publicationDate 2022-07-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114790279-A
titleOfInvention A kind of industrialized production process method of polyglycolic acid oligomer
abstract The invention relates to an industrialized production process method of polyglycolic acid oligomer. The reaction material after mixing raw glycolic acid or glycolic acid ester with a catalyst is first subjected to a normal pressure reaction in a prepolymerization kettle, and the obtained prepolymerized product is then transferred to a reduced The deep polycondensation reaction is carried out in a vacuum state in the membrane reactor, that is, it is completed. Compared with the prior art, the present invention adopts the technology of combining the reaction kettle and the falling film reactor, improves the reaction separation effect and the conversion rate of glycolic acid or glycolic acid ester, improves the product yield, and the molecular weight distribution of the obtained oligomer is relatively high. Narrow, which is conducive to the next step of depolymerization, and can meet the requirements of industrial large-scale production.
priorityDate 2021-01-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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