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filingDate 2022-06-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-09-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114736142-B
titleOfInvention A kind of oil field sewage sterilization and degreasing agent and its synthesis method and application
abstract The invention belongs to the technical field of sewage treatment, and in particular relates to a sterilizing and degreasing agent for oil field sewage, a synthesis method and application. The synthetic method is as follows: adding tertiary amine, dihalobutene, isobutanol, and cupric chloride in a four-necked flask protected by nitrogen, and stirring the temperature for reflux reaction to obtain a crude intermediate product; rotary-evaporating the crude intermediate product to dryness , add water to heat up, stand for stratification, rotate the lower water phase to dryness, and recrystallize to obtain a pure intermediate; add the pure intermediate to a four-necked flask, add ethanol and sodium bisulfite, stir to heat up and reflux for reaction, The crude product is obtained; the crude product is rotary evaporated to dryness and recrystallized to obtain a sterilizing and degreasing agent. The sterilizing and degreasing agent has the characteristics of simple synthesis process, less dosage and low cost; when the concentration is 20mg/L, the sterilization rate can reach 100%; when the concentration is 50mg/L, the oil removal rate can reach more than 99%.
priorityDate 2022-06-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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