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filingDate 2022-04-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_46d19b046ff1443c3cae376ac693ec1c
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publicationDate 2022-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114720609-A
titleOfInvention A method for rapid detection of chlorophthalic acid and dicamba in food based on non-commutation derivatization
abstract The present invention provides a method for rapid detection of chlorophthalic acid and dicamba in food based on non-phase exchange derivatization. Through the technical scheme of the present invention, aiming at the characteristics of easy loss of analytes in the sample pretreatment process, a In the process of processing, the solvent phase is not replaced (hereinafter referred to as no phase change), and the technology of direct injection after derivatization, combined with the multiple reaction monitoring (MRM) mode of triple quadrupole tandem mass spectrometer, has established chlorophthalic acid and dicamba rapid detection method. Compared with the conventional methylesterification derivatization technology, the non-phase derivatization derivatization injection technology greatly simplifies the inspection process, shortens the inspection time, and improves the detection efficiency; , and even in complex matrices such as tea and condiments, the quantification limits of chlorophthalic acid and dicamba can reach 0.01 mg/kg, which meets the requirements of the national standard.
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