http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114720579-A

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filingDate 2021-11-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2022-07-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114720579-A
titleOfInvention Detection method of petroleum hydrocarbons (C6-C9) in soil by headspace-gas chromatography
abstract The invention discloses a method for detecting petroleum hydrocarbons (C6-C9) in soil by headspace-gas chromatography, comprising the following steps: A. Sampling: collecting and preserving soil samples according to the relevant requirements of volatile organic compounds in HJ/T166. Collect 2 parallel samples, put them into sampling bottles, and the sample storage area should be free of organic interference; B. Preparation: Weigh 5g of samples (accurate to 0.01g) into a headspace bottle containing 2g of sodium chloride, and quickly add 5mL of water , close the bottle cap, shake well, and test; C. Standard curve preparation: Accurately draw 100 μL of petroleum hydrocarbon C6-C9 standard working solution with a concentration of 1000 mg/L and dilute to 1 mL with methanol, dilute step by step, and quickly pipette an appropriate amount The standard working solution was put into a headspace bottle corresponding to 5mL of water and 2g of sodium chloride to obtain the following concentration curve points: 0.0ug, 0.5ug, 1.0ug, 5.0ug, 10.0ug, 30.0ug; the petroleum hydrocarbons in the soil (C6- C9) The headspace-gas chromatography detection method has the advantages of simple steps, shortened inspection time and good reproducibility of results.
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