http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114671765-A

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ae2c37bdcb99a76cedc4ad778a3f169a
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C201-08
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-08
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-45
filingDate 2021-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_103d6db65b50b3058b42070bbd66ccd9
publicationDate 2022-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114671765-A
titleOfInvention A kind of ketone musk of safe production and preparation method thereof
abstract The invention discloses a safely produced musk ketone and a preparation method thereof. The preparation raw materials in parts by weight include: 20-40 parts of solid acetyls, 40-80 parts of organic solvent, 54-132 parts of nitric acid, and 30-144 parts of sulfuric acid. share. In the present invention, the solid acetylate is used to replace the liquid acetylate, which can reduce the intensity of the reaction, and the silicon carbide microchannel reactor is used to improve the heat transfer efficiency and make the reaction occur continuously. The ratio of raw materials to nitric acid and sulfuric acid is optimized, and on the basis of producing qualified ketone musk, raw materials are saved, energy waste is reduced, and the reaction safety factor is improved.
priorityDate 2021-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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