http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114634441-B
Outgoing Links
| Predicate | Object |
|---|---|
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D209-52 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D209-52 |
| filingDate | 2022-05-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| grantDate | 2022-07-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationDate | 2022-07-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-114634441-B |
| titleOfInvention | A kind of method for synthesizing 6,6-dimethyl-3-azabicyclo[3,1,0]hexane |
| abstract | The invention discloses a new method for synthesizing 6,6-dimethyl-3-azabicyclo[3,1,0]hexane; it starts with ethyl 3-methyl-2-butenoate The starting material is subjected to Michael addition, halogenation, cyclization, deesterification, hydrolysis, and ring closure with ethyl cyanoacetate to obtain caronic anhydride, and caronic anhydride is subjected to aminolysis and reduction to obtain 6,6-dimethyl- 3-azabicyclo[3,1,0]hexane I; the advantages of the present invention: the technological process is simple, the dangerous process is free, the raw materials are cheap and easy to obtain, and compared with the traditional process using ethyl chrysanthemate as the starting material, the method is more efficient. Green, low production energy consumption and cost, suitable for industrial production. |
| priorityDate | 2022-05-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 91.