http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114591358-A

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filingDate 2021-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bb8f0ff49d586066cc44e32956dea696
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_405640bfe8450da88ffb614fe3417a53
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publicationDate 2022-06-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114591358-A
titleOfInvention A kind of preparation method of methacryloyloxypropyl triketoximinosilane
abstract The invention relates to the technical field of preparation of ketoximinosilane, in particular to a preparation method of methacryloyloxypropyltriketooximosilane, comprising the following steps: (1) preparing methacryloyloxypropyltrialkoxy Silane, polymerization inhibitor and catalyst are put into a reaction kettle protected by an inert gas, and the heating temperature is 100-160 °C; (2) In the reaction kettle, according to the molar ratio of the chemical reaction formula, an excess of ketoxime R 1 R 2 is added dropwise. C=NOH, continue stirring for 3 to 8 hours after the dropwise addition, and recover methanol; (3) after the reaction, remove excess ketoxime, add a decolorizing agent to decolorize, and filter to obtain methacryloyloxypropyltrione Oximinosilane products. The preparation method of the invention prepares methacryloxypropyl tributyl ketoxime silane through one-step reaction, the yield of methacryloxypropyl tributyl ketoxime silane is high, the reaction selectivity is high, and the preparation method is stable, It can meet the needs of industrial scale production.
priorityDate 2021-11-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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