http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114573626-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_1c0bef891770d12d70a3aae5808618f5 |
| classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02E60-10 |
| classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-0805 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F7-0827 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F7-08 |
| filingDate | 2020-12-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8da3fe42bbe351980e36b8761e6514da http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_1e93012003377c0633532ff992d988d1 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c86eae589a7dc37419978d3ab58a8bd9 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_82d49239f90e8f073e617128c51fb63b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_30d9ef68846da80f1341947c07585ded http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0e4b167cb5be35998e09f23104f034e0 |
| publicationDate | 2022-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-114573626-A |
| titleOfInvention | A kind of synthetic method of tetravinylsilane |
| abstract | The invention discloses a method for synthesizing tetravinylsilane, which comprises the following steps: 1. Silane is added dropwise to a raw material solution for reaction, wherein the raw material solution is a tetrahydrofuran solution of vinylmagnesium chloride or a tetrahydrofuran solution of vinylmagnesium bromide , the reaction temperature is controlled at 30 ℃ ~ 60 ℃; 2. After the reaction is completed, add alcohol to the reaction solution to carry out the quenching reaction, the quenching reaction temperature is controlled below 30 ℃, and the organic layer is separated after the reaction is completed; 3. The organic layer is successively dried and rectified to obtain the product tetravinylsilane. The invention has the advantages of simple operation steps, few reaction steps, easy purification, and high purity of the obtained tetravinylsilane. |
| priorityDate | 2020-12-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.