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filingDate 2022-01-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2022-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114534761-A
titleOfInvention A kind of preparation method of nickel-doped graphitic carbon nitride photocatalyst
abstract The invention discloses a method for preparing a nickel-doped graphitic carbon nitride photocatalyst. The specific steps of the method are as follows: (1) dissolving nickel nitrate in a beaker containing deionized water, then adding melamine for ultrasonication; (2) dissolving the ultrasonic The suspension was transferred to a water bath while heating and stirring until the water was completely evaporated to dryness, and then placed in an oven to dry; 3. Grind the dried solid into a uniform powder, pour it into a crucible with a lid, and place it in a muffle furnace for calcination ; ④ After the reaction, take out the sample and grind it into powder to obtain nickel-doped graphite phase carbon nitride material. The nickel-doped graphitic carbon nitride material synthesized by the invention exhibits a graphite-like structure, has a large specific surface area, and has a good response to visible light, and can be used as a photocatalyst for the degradation of printing and dyeing wastewater. The photodegradation rate of the dye is 95%, which is characterized by the advantages of low equipment cost, mild reaction conditions and simple reaction process. The method mainly adopts a one-pot synthesis method.
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