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filingDate 2022-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a535d7e9ea2ab67ff63021fe2334d2a9
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publicationDate 2022-05-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114516636-A
titleOfInvention A method for preparing transition metal carbide nanoarrays by transient high temperature thermal shock carbon template
abstract The invention discloses a method for preparing transition metal carbide nano-arrays with instantaneous high temperature thermal shock carbon template, comprising the following steps: (1) depositing vertical graphene (VG) nano-sheets on the surface of a substrate to obtain VG nano-sheets with an array structure (2) Hydrophilic treatment is performed on the VG nanosheets with an array structure to obtain hydrophilic VG nanosheets; (3) A transition metal source and an oxygen source are used as precursors to deposit nanometers on the surface of the hydrophilic VG nanosheets. transition metal oxide film; (4) using the instantaneous high temperature thermal shock technology to process the transition metal oxide film supported on the surface of VG nanosheets to obtain metal carbides with array morphology; the current is 0-20A, and the voltage is 40-80V , the processing time is 20 ~ 100ms. The preparation method of the invention takes an extremely short technological process, and the material has a unique layer, a high specific surface area, a controllable morphology and a single component, and can expose a large number of active sites.
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