http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114316171-A
Outgoing Links
| Predicate | Object |
|---|---|
| assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d890ad239375a780e6827d3407f15ef3 |
| classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G12-08 |
| filingDate | 2022-01-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5d24054f71fdf927a22d6e49b39f7b2c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b53c6720132f6fad524186c5a363365e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_369af72fc961d9400ae489ca0daf2ba4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4680854ee7668f024d91e7b2edf8d77b |
| publicationDate | 2022-04-12-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| publicationNumber | CN-114316171-A |
| titleOfInvention | Preparation method of novel acylhydrazone bond gel through one-step crosslinking polymerization |
| abstract | The invention provides a preparation method of novel acylhydrazone bond gel by one-step crosslinking polymerization. The method is characterized in that 1,3, 5-benzene trimethyl acyl chloride is used as a starting material and reacts with absolute ethyl alcohol to generate triethyl trimesate, and then the triethyl trimesate reacts with hydrazine hydrate to generate trimesoyl hydrazide. And finally, adopting trimesoyl hydrazine and aldehyde as organic monomers to construct a module, taking dimethyl sulfoxide as a solvent medium according to the Schiff base reaction principle and acylhydrazone covalent bonds as cross-linking points, and rapidly and directly synthesizing a series of novel acylhydrazone bond polymer gels at room temperature in one step. Compared with the existing preparation method of the acylhydrazone bond gel material, the novel acylhydrazone bond gel is completed through one-step crosslinking polymerization of organic monomers of hydrazide and aldehyde, the process that the prior acylhydrazone bond gel material is firstly designed and synthesized into a gel factor and then a crosslinking group is searched is omitted, and the design concept is more advanced and novel. The synthesis method is simple, low in cost, mild in condition, high in reaction rate and yield, and has good development and application potential in the aspect of intelligent materials. |
| isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114907278-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114907278-A |
| priorityDate | 2022-01-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
| type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.