http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114262110-A

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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01D5-00
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filingDate 2021-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_eb227583a27c16349f12dc119dee2c9b
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publicationDate 2022-04-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114262110-A
titleOfInvention Integrated synergistic recovery method of sodium sulfate and methanol from methyl pyrimidin-phosphine production wastewater
abstract The invention discloses an integrated synergistic recovery method of sodium sulfate and methanol in methyl pyrimidine production wastewater. The method comprises the following steps: cooling the sodium sulfate wastewater to ‑5 to 10°C for crystallization, and cooling the sodium sulfate wastewater to ‑5 to 10°C for crystallization, and at a temperature of ≤20°C Carry out solid-liquid separation, the obtained sodium sulfate decahydrate is heated, distilled and concentrated, and centrifuged, the obtained anhydrous sodium sulfate crude product is rinsed with sodium sulfate solution, centrifuged, and dried to obtain sodium sulfate solid, which also includes using sodium sulfate solid to water-containing. Methanol was purified to obtain anhydrous methanol. The integrated synergistic recovery method of sodium sulfate and methanol in the waste water of methyl pyrimidine production of the present invention, through the combined treatment of cooling crystallization, low-temperature filtration, distillation concentration, and leaching filtration, can realize zero discharge of waste water, improve the environment, and save energy. It can reduce consumption, and can synergistically recover by-products (sodium sulfate, methanol, xylene, water), which is conducive to improving the economic benefits of enterprises.
priorityDate 2021-12-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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