http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114085375-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G69-14
filingDate 2020-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5d175e29eedb3ab3d0c8c95638a5c34d
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publicationDate 2022-02-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-114085375-A
titleOfInvention A kind of synthetic method of narrow molecular weight distribution polyamide
abstract The invention discloses a method for synthesizing polyamide with narrow molecular weight distribution. The method comprises the steps of adding raw materials including nylon salt, water and diamine into a reaction kettle, raising the temperature to 180-240° C., at 0.2-1.8 MPa. React under pressure for 1.0 to 3.0 hours, release the pressure to normal pressure; then heat up to 240 to 265 ° C, first react at normal pressure for 1.0 to 3.0 hours, and then under pressure of ‑0.04 to ‑0.08MPa, react for 0.5 to 3.0 hours, that is have to. In the method, nylon salt is used as the main reactant, and diamine is introduced as a regulator, which can effectively inhibit the decomposition of nylon salt at high temperature, reduce the polymerization reaction pressure, neutralize the dibasic acid generated by the decomposition of nylon salt, and also play a role in The role of molecular weight regulators can obtain polyamide products with narrower molecular weight distribution, more stable viscosity and better quality.
priorityDate 2020-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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