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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C09D101-14
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08B3-02
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C09D101-14
filingDate 2021-11-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-08-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-08-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113956364-B
titleOfInvention A kind of preparation method of cellulose acetate butyrate
abstract The invention provides a preparation method of cellulose acetate butyrate, which relates to the technical field of cellulose modification. The preparation method specifically includes the following steps: (1) Activation: immersing cellulose in a mixed activation solution of acetic acid and acetic anhydride (2) Esterification and hydrolysis: After mixing the activated cellulose with acetic acid and acetic anhydride, under the catalyzed condition of a solid acid catalyst, carry out an esterification reaction, and then add the esterified cellulose to the Hydrolysis is carried out in acetic acid; (3) purification: the hydrolyzed cellulose is precipitated, filtered, washed and dried to obtain cellulose acetate butyrate; the solid acid catalyst includes catalyst A and catalyst B; the catalyst A is SO 4 2 --ZrO 2 -Fe 2 O 3 catalyst, and the catalyst B is SO 4 2 --ZrO 2 -Al 2 O 3 catalyst. The preparation method is convenient and pollution-free, and can be prepared with high yield and high content of butyryl groups.
priorityDate 2021-11-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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