http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113941120-B
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A62D2203-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A62D2101-40 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A62D3-30 |
classificationIPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A62D101-40 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A62D3-30 |
filingDate | 2021-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-03-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-113941120-B |
titleOfInvention | Digestion method of graphene material |
abstract | The invention belongs to the technical field of graphite material analysis, and particularly relates to a digestion method of a graphene material. The digestion method comprises the following steps: (1) oxidation of graphene: oxidizing graphene to form graphene oxide; (2) modification treatment of graphene oxide: introducing amino groups into the graphene oxide conjugated region; (3) digestion treatment: mixing the modified graphene oxide and hydrofluoric acid, pressurizing to 0.20-0.32MPa at the temperature of 170-200 ℃, maintaining the pressure for 20-60min, then relieving the pressure to normal pressure, reacting for 10-60min at normal pressure, and performing pressurization and pressure relief circulation for 3-5 times, and discharging. Wherein, the pressure relief to normal pressure is as follows: and (5) releasing the pressure to the normal pressure within 10-30 s. The method can efficiently complete the digestion treatment of the graphene, and avoids the influence of the residue of the graphene on the accuracy of the test result. |
priorityDate | 2021-12-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 38.