http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113896698-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D307-12
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D307-12
filingDate 2020-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0af752d8fffd15a80b0b4427b72ab54b
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publicationDate 2022-01-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113896698-A
titleOfInvention A kind of synthetic method of tetrahydrofurfuryl alcohol ethyl ether
abstract The invention discloses a method for synthesizing tetrahydrofurfuryl alcohol ethyl ether. The method is to carry out dehydration reaction between THFA and alkali metal hydroxide in an alkoxide solvent system containing a water agent, and simultaneously separate the water produced by the dehydration reaction. , to obtain an alkoxide product; the alkoxide solvent is C 7 -C 12 aryl alcohol or furan ether; after cooling, the alkoxide product is subjected to condensation reaction with halogenated ethane to obtain a crude ETFE product containing salt; After the salt-containing crude ETFE product is filtered to remove the chloride salt, the ETFE fraction is collected by rectification; the mass content of the obtained ETFE fraction is higher than 98.0% ETFE, the total reaction yield is > 95%, and the solvent in the rectification kettle can be recycled. .
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114213364-A
priorityDate 2020-06-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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