| abstract |
The invention discloses a preparation method and an analysis method of a flat explosive LLM-105 solvate, comprising the following steps: (1) adding LLM-105 raw materials and a solvent into a conical flask, sealing the bottle mouth with a balloon, and placing the LLM-105 raw material and solvent into a conical flask, Heating in a bath, and by magnetic stirring, LLM-105 is completely dissolved; (2) the LLM-105 solution in step (1) is naturally cooled to room temperature to obtain LLM-105 supersaturated solution; (3) LLM-105 The supersaturated solution was placed in a constant temperature incubator for more than a week, and orange needle-like LLM-105 solvate crystals were formed at the bottom of the Erlenmeyer flask. The present invention realizes the synthesis and crystal structure analysis of LLM-105 solvate for the first time. |