abstract |
The invention discloses a preparation method for realizing a bismuth boron-based flexible catalytic electrode in an organic phase. Mix and prepare a plating solution; after ultrasonic cleaning of the base material in deionized water, the base material is then immersed in deionized water, ethanol and acetone in sequence; the flexible base material is immersed in a metal salt solution, and at the same time in borohydride Dip for 2s to complete the activation of the flexible non-conductive substrate, and then rinse it with deionized water and ethanol in turn; immerse the pretreated substrate material into the plating solution prepared in the first step, and take out the electroless plating reaction. The base material, after rinsing with ethanol, the obtained electrode material is the product. According to the present invention, the preparation method is simple, has good universality, low production cost, can change the concentration in a wide range, has good stability, and has low requirements on working environment. |