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filingDate 2021-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-10-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-10-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113831581-B
titleOfInvention A kind of highly elastic radiation-resistant nanofiber aerogel material and preparation method thereof
abstract The invention relates to a high-elasticity radiation-resistant nanofiber aerogel material and a preparation method thereof. The method comprises the following steps: mixing ethyl orthosilicate, phosphoric acid and water uniformly, stirring for 1-24 hours, then adding titanium dioxide nano-powder and continuing to stir 1~12h, after ultrasonic treatment, a composite hydrolyzate is obtained; the polyvinyl alcohol aqueous solution and the composite hydrolyzate are mixed with water and stirred for 1~12h, and then the precursor solution is electrospun to obtain a hybrid nanofiber membrane; The nanofiber membrane is heat-treated; the heat-treated hybrid nanofiber membrane, ethyl orthosilicate, boric acid and aluminum chloride are added to water, and a graphene oxide solution is added for high-speed stirring to obtain a homogeneous dispersion; The phase dispersion liquid is sequentially frozen, freeze-dried and post-treated to obtain a highly elastic radiation-resistant nanofiber aerogel material. The material prepared by the invention has high elasticity and excellent radiation resistance, temperature resistance and high temperature heat insulation performance.
priorityDate 2021-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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