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filingDate 2021-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0b3a89b72c36c77c3c70ed0e26c13986
publicationDate 2021-11-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113675398-A
titleOfInvention A kind of lithium ion battery negative electrode material and preparation method thereof
abstract The invention discloses a preparation method of NiMnO 3 /MnCo 2 S 4 composite material of lithium ion battery negative electrode material: (1) N,N-dimethylformamide and ethylene glycol are mixed uniformly, and then the molar ratio is 1 The soluble nickel salt, manganese salt and isophthalic acid of 1 are added to the mixed solvent successively, and the ultrasonic mixing is uniform; (2) the mixed solution in the step (1) is transferred to the autoclave, and the solvothermal method is carried out at 180-200 ℃. The reaction is carried out for 12-24h, followed by washing the product for several times, and heat treatment at 300-400° C. for 1-2h to obtain flower-shaped NiMnO 3 ; (3) NiMnO 3 is dissolved in ethanol, stirred uniformly, and then a soluble manganese salt is added , cobalt salt and thiourea were mixed uniformly by ultrasonic, then acetylacetone was added, ultrasonically mixed uniformly and then transferred to a high pressure reactor, and reacted at 200 to 220 ° C for 6 to 12 hours; the product was washed with ethanol and deionized for many times to obtain NiMnO 3 /MnCo 2 S 4 composite.
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