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publicationDate 2021-11-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113624798-A
titleOfInvention Method for measuring content of gutta-percha by quantitative nuclear magnetic resonance hydrogen spectrum
abstract The invention belongs to the technical field of analysis, and particularly relates to a method for determining the content of gutta-percha by quantitative nuclear magnetic resonance hydrogen spectrum. The method comprises the steps of eliminating the interference of impurities in a solvent and hydrogen peaks of the solvent and the signal interference between a detected component and the impurities by setting parameters in a specific detection process, setting a pulse flip angle and a relaxation time of a nuclear magnetic resonance spectrometer by a longitudinal relaxation time T1 value, and detecting a nuclear magnetic hydrogen spectrum of a solution to be detected by the nuclear magnetic resonance spectrometer. Finally, the determination integration is accurate, and the detection result has good reproducibility. The method is quick, and only a high-purity reference substance is needed as a reference, and a standard substance of a target test substance is not needed to be used as an external standard. The method can rapidly, accurately and stably determine the content of the gutta-percha. The error of direct weighing after conventional application and purification is overcome. The method has the advantages of low cost, simple operation, accurate result, no need of a gutta-percha standard substance during sample testing, good repeatability and the like, and can quickly evaluate the content of the gutta-percha in the eucommia ulmoides extract.
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