http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113563394-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_cb351a5a4e03ee3773bd0df5dbae9ac3 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H1-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H1-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07H5-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H5-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H1-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H1-00 |
filingDate | 2021-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_60ba462a0a33d566e776ca6e8ce9d57b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ce233188deed23227c43eff05d87d07d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_07d22ac130b9187fb63c074acbc0fe46 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_15dd8a415fb6dd6b29bb056c9637d94a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f1846b0f03250b88ffaaafaf914a48f7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9594932003de396370f819a3dc5e358a |
publicationDate | 2021-10-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-113563394-A |
titleOfInvention | A kind of preparation method of chitosan oligosaccharide monomer |
abstract | The invention discloses a preparation method of chitosan oligosaccharide monomer. The present invention pretreats the chitosan oligosaccharide solution, so that the high-concentration chitosan oligosaccharide solution is graded and precipitated in 80-90% ethanol solution, the chitosan oligosaccharide with a high degree of polymerization is precipitated, and the chitosan oligosaccharide with a small degree of polymerization remains in the supernatant In the liquid, the precipitation is processed for the second time, the supernatants obtained from the two times are combined, concentrated by rotary evaporation, and the concentrated solution is freeze-dried to obtain a crude chitosan oligosaccharide with a high polymerization degree of 1-5. Then carry out cation exchange chromatographic separation, adopt staged isocratic elution, one eluent concentration only elutes one degree of polymerization of chitosan oligosaccharide, the separation process does not need to be detected, the purity of the obtained chitosan oligosaccharide monomer reaches more than 90%, and the yield is to the gram level. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113845605-B http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113845605-A |
priorityDate | 2021-07-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 40.