http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113533630-A
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_780642ba0df07159e802b3f2ed213a3e |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N31-16 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N31-16 |
filingDate | 2021-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5908e0a25c4dddf5a4833b1d0fbcc5ab http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6f5917526ced7edb2492da1b08a2257d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6404d06629cae2ce5e91aee0ad464ab3 |
publicationDate | 2021-10-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-113533630-A |
titleOfInvention | Method for industrially detecting sulfur content in combustible solid acenaphthene |
abstract | The invention discloses a method for industrially detecting the sulfur content in combustible solid acenaphthene. The detection method comprises the following steps: s1, mixing an acenaphthene sample to be detected, magnesium oxide and a mixed flux with a crucible, and then adding absolute ethyl alcohol until the mixture is solid; the mixed flux is a mixture of anhydrous sodium carbonate and magnesium oxide; s2, igniting the solid, and carrying out melting roasting until the solid is flameless; s3, washing the product obtained in the step S2 by a sodium carbonate solution, and filtering; s4, transferring the filtrate obtained in the step S3 to a volumetric flask, and diluting with deionized water to a constant volume; s5, transferring part of the solution in the step S4, adjusting the pH to 5.5-6.5, adding absolute ethyl alcohol and 3-4 drops of C 6 Na 2 O 6 Indicator, then BaCl 2 And titrating the standard solution until the solution is suddenly changed into red, and obtaining the content of sulfur in the solution according to the formula W% ═ 32 XCXV, so as to obtain the content of sulfur in the acenaphthene sample. The invention does not use heating equipment such as a muffle furnace and the like, does not adopt other large-scale detecting instruments, and simply and conveniently measures the sulfur content in the solid. |
isCitedBy | http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114487225-A |
priorityDate | 2021-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 30.