http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113512016-A

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filingDate 2021-08-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_768b34dad49afcbcb5e2ecb5afbf6aae
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publicationDate 2021-10-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113512016-A
titleOfInvention A one-pot method for preparing 5-hydroxymethylfurfural from carbohydrates catalyzed by lithium bromide molten salt hydrate-acetone system
abstract The invention discloses a method for preparing 5-hydroxymethyl furfural by a one-pot method of carbohydrate-catalyzed lithium bromide molten salt hydrate-acetone system. The method comprises the following steps: mixing carbohydrates, lithium bromide molten salt hydrate and acetone to carry out a hydrothermal reaction, and after sufficient reaction, a reaction solution of reducing sugar and 5-hydroxymethylfurfural in high yield can be obtained. Phosphoric acid or aluminum chloride is also added during the reaction. In the present invention, the two-phase system constructed by lithium bromide molten salt hydrate and acetone can efficiently catalyze the conversion of cellulose by one-pot method, and obtain high-yield 5-hydroxymethylfurfural under the catalysis of aluminum chloride. Moreover, the invention has the advantages of simple process, low cost, fast conversion speed and high selective conversion.
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priorityDate 2021-08-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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