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filingDate 2021-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2021-10-08-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113479937-A
titleOfInvention A kind of method for preparing spherical iron oxide
abstract The invention discloses a method for preparing quasi-spherical iron oxide. The preparation method includes adjusting the acidity of a mixed rare earth solution containing impurity iron; using a compound extraction solvent to extract and separate iron and mixed rare earth elements in cascade; The raffinate is discharged from the raffinate, and the composite extractant extracts iron to obtain a phase A microemulsion. The phase A microemulsion enters the stripping section; the phase B microemulsion is added to the stripping section as washing liquid and stripping liquid. Set it until no more precipitation is formed, filter, wash and dry to obtain the ferric hydroxide precursor; the B-phase microemulsion is obtained by mixing the composite extraction solvent and the alkaline solution; the ferric hydroxide precursor is roasted to obtain the ferric oxide; this method can be In the rare earth extraction and separation process, the iron removal wastewater is fully utilized to achieve the purpose of environmental protection. In addition, the loss of iron elements in the whole process of preparation is small, and the prepared iron oxide has high purity, small particle size of iron oxide powder and good dispersibility.
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