http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113429555-B

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G64-30
filingDate 2021-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-07-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-07-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113429555-B
titleOfInvention Polycarbonate diol and preparation method thereof
abstract The invention relates to the technical field of fine chemicals, in particular to a polycarbonate diol and a preparation method thereof. The preparation method of the polycarbonate diol includes the following steps: mixing polyol, carbonate and sodium alkoxide catalysts, carrying out a transesterification polycondensation reaction to obtain a product intermediate; mixing the product intermediate and an acidic reagent, heating at 160° C. The reaction is carried out at an ambient temperature of ~200° C., and then pressure-filtered at an ambient temperature of not less than 100° C. to remove the solid; the acidic reagent is selected from an aqueous phosphoric acid solution or an aqueous hydrochloric acid solution. The preparation method of the invention is simple to operate, convenient, energy-saving and environmentally friendly, greatly reduces labor and material costs in industrial production, saves production costs, and has better catalyst removal effect. The catalyst content is low.
priorityDate 2021-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 48.