http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113337836-A

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filingDate 2021-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5d5ea0f3d60a88e92f5a37877f75799c
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publicationDate 2021-09-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113337836-A
titleOfInvention A kind of preparation method of electrochemical oxidation of cyclohexanone to synthesize adipic acid
abstract The invention relates to a preparation method for synthesizing adipic acid by electrochemical oxidation of cyclohexanone. Conducting with the plasma gas, step 2 is to conduct electrolysis while introducing the plasma gas into the electrolyte, and after the electrolyzed electrolyte is filtered and dried, the adipic acid product is obtained; the present invention is an electrochemical reaction system. Nitrogen-plasma gas is introduced into the cyclohexanone, which can not only prevent cyclohexanone from contacting with air and be oxidized by oxygen in the air, but also protect Mn 2+ from being oxidized into MnO 2 , MnO 4 2- high-valence substances, and inhibit solid MnO 2 The formation of ions can avoid the occurrence of side reactions and improve the electrolysis efficiency; the invention uses the DSA anode with high electrocatalytic performance and strong corrosion resistance, which can speed up the electrolysis reaction rate and improve the final yield of the product.
priorityDate 2021-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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