http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113292425-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-48
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filingDate 2021-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_73749407af49572f2aa0f5d397a5aa35
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publicationDate 2021-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113292425-A
titleOfInvention Production method of bis (2-propyl) heptyl terephthalate
abstract The application relates to the field of plasticizers, and particularly discloses a production method of bis (2-propyl) heptyl terephthalate. A method for producing bis (2-propyl) heptyl terephthalate comprises the following steps: step 1, preparing raw materials, namely weighing 2-propyl-1-heptanol, terephthalic acid and tetraisopropyl titanate, wherein the molar ratio of the 2-propyl-1-heptanol to the terephthalic acid is 2.0-4.0: 1, the dosage of the tetraisopropyl titanate is 0.01 to 0.20 percent of the total mass of the 2-propyl-1-heptanol and the terephthalic acid; step 2, esterification reaction, namely mixing and stirring the raw materials prepared in the step 1 at the temperature of 170-245 ℃ for 2-5 hours to obtain a crude product; step 3, post-treatment, namely neutralizing the crude product and washing the neutralized crude product for 1 to 3 times; and 4, decoloring, namely cooling the product subjected to the post-treatment in the step 3, decoloring and filtering to obtain a final product. The production method has the advantages of reducing the using amount of the catalyst and improving the production safety of the bis (2-propyl heptyl) terephthalate.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-114456062-A
priorityDate 2021-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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