http://rdf.ncbi.nlm.nih.gov/pubchem/patent/CN-113277956-B
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J31-069 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J31-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-03 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C231-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C233-15 |
filingDate | 2021-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-11-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2022-11-04-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | CN-113277956-B |
titleOfInvention | A method for synthesizing amide compounds using non-polluting coupling agent |
abstract | The invention discloses a method for synthesizing amide compounds by using a non-polluting coupling agent, and relates to the technical field of organic synthesis. In view of the problems of long stirring and low heating efficiency in the prior art, the following solutions are proposed, including the following Steps: take aromatic carboxylic acid and aliphatic amine as base materials, mix and stir with improved coupling agent at room temperature, and assisted by microwave irradiation, and separate and purify after the reaction to obtain synthetic amide compounds. Under the coordination of microwave irradiation, the invention promotes the synthesis of aromatic carboxylic acid and aliphatic amine, greatly reduces the reaction time, improves the synthesis efficiency and the amine conversion rate, and contributes to the improvement of production efficiency and the advancement of synthesis technology. , and the improved coupling agent used has high microwave absorption efficiency, further promotes the reaction, and improves the efficiency of the compound reaction, and the raw materials used are simple to obtain, non-polluting, and environmentally friendly. |
priorityDate | 2021-06-03-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 37.