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filingDate 2021-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2022-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113234256-B
titleOfInvention Preparation method of double-crosslinking flame-retardant composite aerogel
abstract The invention discloses a preparation method of a double-crosslinking flame-retardant composite aerogel, which comprises the following steps: 1) amino protonation treatment of chitosan: placing chitosan in an acid solution to obtain a chitosan solution with amino groups on a molecular chain protonated; 2) preparing the composite aerogel: dispersing nano montmorillonite into mixed suspension of nano cellulose and chitosan, adding a cross-linking agent, stirring to obtain mixed solution, pouring the mixed solution into a mould, freezing, and performing cross-linking reaction to obtain composite aerogel; 3) a double cross-linking step: and (3) soaking the obtained composite gel in a mixed solution of a polyphosphate solution and a transition metal chloride solution for treatment, and freeze-drying to obtain the double-crosslinking flame-retardant composite aerogel. The composite aerogel material obtained by the invention has excellent flame retardant property, mechanical property and smoke suppression property; the method has the advantages of low raw material source, low production cost and wide application.
priorityDate 2021-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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