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filingDate 2021-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_8c60686261267b9be8bba6f53dadd5c5
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publicationDate 2021-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113201400-A
titleOfInvention A kind of production technology that is conducive to the preparation of spice by extraction method
abstract The invention discloses a production process for preparing spices by an extraction method. The production process is as follows: step 1: material preparation: the materials include safrole, potassium hydroxide solution, lye, p-aminobenzenesulfonic acid, sulfuric acid, Sodium dichromate, benzene, ethanol, saturated brine; Step 2: adding safrole in the steamer, and adding potassium hydroxide solution to the steamer, heating up, cooling, and discarding the lye, and distillation to obtain isocyanide. safrole; step 3: adding isosafrole to the reaction kettle, adding sodium dichromate, water, p-aminobenzenesulfonic acid to the reaction kettle, stirring to make the materials evenly mixed, and adding a sulfuric acid solution dropwise , after the dropwise addition is completed, the temperature is raised to 55-60 ℃ by the reaction, the temperature is kept for 30-40min under stirring, and then cooled down; the beneficial effects of the present invention are: the preparation process is simplified, and the efficiency of the production and processing of spices is improved; extraction, washing , distillation and crystallization make the aroma of the prepared spices more pure.
priorityDate 2021-04-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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