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filingDate 2021-04-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_895e72c389803f07760e1a4a2bdf38f6
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publicationDate 2021-08-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber CN-113198437-A
titleOfInvention A method for preparing fullerene solid-phase microextraction probe coating based on solvent evaporation and recrystallization technology
abstract The invention discloses a method for preparing a fullerene solid-phase micro-extraction probe coating based on a solvent evaporation and recrystallization technology. The deposition of a certain amount of unburned carbon; the pretreated stainless steel wire is immersed in the prepared fullerene-carbon disulfide supersaturated solution. During the heating process, with the evaporation of the carbon disulfide solvent, the fullerene material recrystallizes on the surface of the stainless steel wire ; Repeat the recrystallization step until the desired thickness of the SPE probe coating is obtained; Assemble the prepared fullerene-deposited stainless steel wire into the SPE hollow needle to obtain a fullerene SPE probe, before use Aging treatment. The method has simple operation steps, low cost, and high sensitivity for extraction and analysis of the prepared coating, and has broad application prospects.
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